GB1236885A - Method of making multi-wall capsules - Google Patents

Method of making multi-wall capsules

Info

Publication number
GB1236885A
GB1236885A GB4747669A GB4747669A GB1236885A GB 1236885 A GB1236885 A GB 1236885A GB 4747669 A GB4747669 A GB 4747669A GB 4747669 A GB4747669 A GB 4747669A GB 1236885 A GB1236885 A GB 1236885A
Authority
GB
United Kingdom
Prior art keywords
capsules
wall
acid
alkali
wall capsules
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB4747669A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Fujifilm Holdings Corp
Original Assignee
Fuji Photo Film Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Fuji Photo Film Co Ltd filed Critical Fuji Photo Film Co Ltd
Publication of GB1236885A publication Critical patent/GB1236885A/en
Expired legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
    • B01J13/02—Making microcapsules or microballoons
    • B01J13/06—Making microcapsules or microballoons by phase separation
    • B01J13/10—Complex coacervation, i.e. interaction of oppositely charged particles

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Preparation (AREA)

Abstract

1,236,885. Multi-wall capsules. FUJI PHOTO FILM CO. Ltd. 26 Sept., 1969 [28 Sept., 1968], No. 47476/69. Heading B8C. Multi-wall capsules, each consisting of one or more single-wall capsules enclosed within one or more further polymeric walls are prepared by dispersing single wall capsules in an aqueous solution of a water-soluble, film-forming, high molecular weight material having hydroxyl, acid or basic groups, and adding portions (e.g. drops, or extruded portions) of the dispersion to an aqueous solution of a hardener for the said high molecular weight material. If desired, the procedure may be repeated to give capsules having 3 or more wall layers. Specified high M.W. materials (together with the appropriate hardener) are: sodium alginate (Ca<SP>++</SP>, Al<SP>+++</SP>, acid); carageenin (Ca<SP>++</SP>); dextran (Ca<SP>++</SP>, Ba<SP>++</SP>); carboxy methyl-cellulose and -starch (Al<SP>++</SP><SP>+</SP>, Fe<SP>++</SP><SP>+</SP>, Cu<SP>+</SP> <SP>+</SP>); collagen (alkali), polyvinyl alcohol (borax) ; polyvinyl methyl ether/ maleic anhydride copolymer; agar (tannic acid with cooling); milk casein (Ca<SP>++</SP>, acid); chitosan oxalate (alkali) and glucomannan (Ca<SP>++</SP>, alkali).
GB4747669A 1968-09-28 1969-09-26 Method of making multi-wall capsules Expired GB1236885A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP7063768 1968-09-28

Publications (1)

Publication Number Publication Date
GB1236885A true GB1236885A (en) 1971-06-23

Family

ID=13437340

Family Applications (1)

Application Number Title Priority Date Filing Date
GB4747669A Expired GB1236885A (en) 1968-09-28 1969-09-26 Method of making multi-wall capsules

Country Status (1)

Country Link
GB (1) GB1236885A (en)

Cited By (54)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2386345A1 (en) * 1977-04-08 1978-11-03 Kureha Chemical Ind Co Ltd PROCESS FOR OBTAINING MICROCAPSULES OF AGRICULTURAL CHEMICALS CONTAINING ORGANOPHOSPHORIC ACID DERIVATIVES
FR2452285A1 (en) * 1979-03-28 1980-10-24 Damon Corp METHOD OF ENCAPSULATION OF A LIVABLE TISSUE OR OF A BIOLOGICALLY ACTIVE MATERIAL TO BE IMPLANTED, AND CAPSULES OBTAINED
FR2521428A1 (en) * 1982-02-18 1983-08-19 Ceca Sa Gastro:resistant capsules - mfd. from alginic acid or water-insoluble alginate
EP0088552A1 (en) * 1982-02-26 1983-09-14 THE UNITED STATES OF AMERICA as represented by the Secretary UNITED STATES DEPARTMENT OF COMMERCE Encapsulation by entrapment within polyhydroxy polymer borates
EP0097093B1 (en) * 1982-06-14 1986-09-03 Bernard Pesche Manufacturing process for a product for the control of animal pests
US4895725A (en) * 1987-08-24 1990-01-23 Clinical Technologies Associates, Inc. Microencapsulation of fish oil
EP0391803A1 (en) * 1989-04-07 1990-10-10 L'oreal Process for preparing alginate capsules particularly useful for cosmetics, apparatus for performing said process and cosmetic composition containing said capsules
US5204111A (en) * 1989-04-07 1993-04-20 L'oreal Process for the preparation of alginate capsules, apparatus for producing said capsules and cosmetic compositions containing said capsules
US5541155A (en) 1994-04-22 1996-07-30 Emisphere Technologies, Inc. Acids and acid salts and their use in delivery systems
US5578323A (en) 1992-06-15 1996-11-26 Emisphere Technologies, Inc. Proteinoid carriers and methods for preparation and use thereof
US5601846A (en) 1992-06-15 1997-02-11 Emisphere Technologies, Inc. Proteinoid microspheres and methods for preparation and use thereof
US5629020A (en) 1994-04-22 1997-05-13 Emisphere Technologies, Inc. Modified amino acids for drug delivery
US5643957A (en) 1993-04-22 1997-07-01 Emisphere Technologies, Inc. Compounds and compositions for delivering active agents
US5650386A (en) 1995-03-31 1997-07-22 Emisphere Technologies, Inc. Compositions for oral delivery of active agents
US5693338A (en) 1994-09-29 1997-12-02 Emisphere Technologies, Inc. Diketopiperazine-based delivery systems
US5709861A (en) 1993-04-22 1998-01-20 Emisphere Technologies, Inc. Compositions for the delivery of antigens
US5750147A (en) 1995-06-07 1998-05-12 Emisphere Technologies, Inc. Method of solubilizing and encapsulating itraconazole
US5788991A (en) * 1993-04-01 1998-08-04 Novartis Corporation Coated microparticle agglomerates
US5792451A (en) 1994-03-02 1998-08-11 Emisphere Technologies, Inc. Oral drug delivery compositions and methods
US5804688A (en) 1997-02-07 1998-09-08 Emisphere Technologies, Inc. Compounds and compositions for delivering active agents
US5820881A (en) 1995-04-28 1998-10-13 Emisphere Technologies, Inc. Microspheres of diamide-dicarboxylic acids
US5824345A (en) 1995-06-07 1998-10-20 Emisphere Technologies, Inc. Fragrances and flavorants
US5863944A (en) 1997-04-30 1999-01-26 Emisphere Technologies, Inc. Compounds and compositions for delivering active agents
US5866536A (en) 1995-03-31 1999-02-02 Emisphere Technologies, Inc. Compounds and compositions for delivering active agents
US5876710A (en) 1997-02-07 1999-03-02 Emisphere Technologies Inc. Compounds and compositions for delivering active agents
US5879681A (en) 1997-02-07 1999-03-09 Emisphere Technolgies Inc. Compounds and compositions for delivering active agents
US5939381A (en) 1997-02-07 1999-08-17 Emisphere Technologies, Inc. Compounds and compositions for delivering active agents
US5962710A (en) 1997-05-09 1999-10-05 Emisphere Technologies, Inc. Method of preparing salicyloylamino acids
US5965121A (en) 1995-03-31 1999-10-12 Emisphere Technologies, Inc. Compounds and compositions for delivering active agents
US5990166A (en) 1997-02-07 1999-11-23 Emisphere Technologies, Inc. Compounds and compositions for delivering active agents
US5989539A (en) 1995-03-31 1999-11-23 Emisphere Technologies, Inc. Compounds and compositions for delivering active agents
US6001347A (en) 1995-03-31 1999-12-14 Emisphere Technologies, Inc. Compounds and compositions for delivering active agents
EP0970623A2 (en) * 1998-07-08 2000-01-12 K.D. Pharma Bexbach GmbH Micro-encapsulated unsaturated fatty acids or derivatives with two polymer layers
US6051258A (en) 1995-06-07 2000-04-18 Emisphere Technologies, Inc. Proteinoid emulsions and methods for preparation and use thereof
US6060513A (en) 1997-02-07 2000-05-09 Emisphere Technologies, Inc. Compounds and compositions for delivering active agents
US6071510A (en) 1995-03-31 2000-06-06 Emisphere Technologies, Inc. Modified amino acids and compositions comprising the same for delivering active agents
US6071538A (en) 1992-06-15 2000-06-06 Emisphere Technologies, Inc. Oral delivery composition comprising supramolecular complex
US6084112A (en) 1995-09-11 2000-07-04 Emisphere Technologies, Inc. Method for preparing ω-aminoalkanoic acid derivatives from cycloalkanones
US6090958A (en) 1995-03-31 2000-07-18 Emisphere Technologies, Inc. Compounds and compositions for delivering active agents
US6126936A (en) * 1995-03-10 2000-10-03 Biohybrid Technologies Llc Microcapsules and composite microreactors for immunoisolation of cells
US6221367B1 (en) 1992-06-15 2001-04-24 Emisphere Technologies, Inc. Active agent transport systems
WO2001030146A1 (en) * 1999-10-22 2001-05-03 3M Innovative Properties Company Encapsulated active material immobilized in hydrogel microbeads
US6242495B1 (en) 1997-02-07 2001-06-05 Emisphere Technologies, Inc. Compounds and compositions for delivering active agents
WO2001064329A1 (en) * 2000-02-29 2001-09-07 Rainer Pommersheim Microcapsule, in particular, for immobilizing organic or inorganic solids, liquids and/or gases
US6287558B1 (en) 1997-08-01 2001-09-11 Biohybrio Technologies Llc Devices containing cells or tissue and an agent that inhibits damage by a host cell molecule
US6331318B1 (en) 1994-09-30 2001-12-18 Emisphere Technologies Inc. Carbon-substituted diketopiperazine delivery systems
US6375983B1 (en) 1996-06-14 2002-04-23 Emisphere Technologies, Inc. Microencapsulated fragrances and method for preparation
WO2005013941A1 (en) * 2003-08-06 2005-02-17 Fondazione Carlo E Dirce Callerio Onlus Polysaccharide double-layer microcapsules as carriers for biologically active substance oral administration
WO2009094859A1 (en) 2008-01-25 2009-08-06 Rj Reynolds Tobacco Company Process for manufacturing breakable capsules useful in tobacco products
WO2010044834A2 (en) 2008-10-17 2010-04-22 Appleton Papers Inc. A fragrance-delivery composition comprising boron and persulfate ion-crosslinked polyvinyl alcohol microcapsules and method of use thereof
US8686154B2 (en) 1997-02-07 2014-04-01 Emisphere Technologies, Inc. Compounds and compositions for delivering active agents
EP2906050B1 (en) 2012-10-09 2018-04-25 Societe D Exploitation De Produits Pour Les Industries Chimiques Seppic Dietary compositions comprising capsules obtained by coacervation without the use of toxic cross-linking agents
CN108283627A (en) * 2018-04-11 2018-07-17 广西壮族自治区农业科学院农产品加工研究所 A method of preparing starch capsule by major ingredient of hair sweet potato starch
US10143212B2 (en) 2005-04-26 2018-12-04 Massey University Lipid encapsulation

Cited By (80)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2386345A1 (en) * 1977-04-08 1978-11-03 Kureha Chemical Ind Co Ltd PROCESS FOR OBTAINING MICROCAPSULES OF AGRICULTURAL CHEMICALS CONTAINING ORGANOPHOSPHORIC ACID DERIVATIVES
FR2452285A1 (en) * 1979-03-28 1980-10-24 Damon Corp METHOD OF ENCAPSULATION OF A LIVABLE TISSUE OR OF A BIOLOGICALLY ACTIVE MATERIAL TO BE IMPLANTED, AND CAPSULES OBTAINED
JPS55157502A (en) * 1979-03-28 1980-12-08 Damon Corp Live tissue encapsulation and tissue transplantation
JPS6239131B2 (en) * 1979-03-28 1987-08-21 Damon Biotech Inc
FR2521428A1 (en) * 1982-02-18 1983-08-19 Ceca Sa Gastro:resistant capsules - mfd. from alginic acid or water-insoluble alginate
EP0088552A1 (en) * 1982-02-26 1983-09-14 THE UNITED STATES OF AMERICA as represented by the Secretary UNITED STATES DEPARTMENT OF COMMERCE Encapsulation by entrapment within polyhydroxy polymer borates
EP0097093B1 (en) * 1982-06-14 1986-09-03 Bernard Pesche Manufacturing process for a product for the control of animal pests
US4895725A (en) * 1987-08-24 1990-01-23 Clinical Technologies Associates, Inc. Microencapsulation of fish oil
US5139783A (en) * 1989-04-07 1992-08-18 L'oreal Process for the preparation of alginate capsules, apparatus for producing said capsules and cosmetic compositions containing said capsules
FR2645439A1 (en) * 1989-04-07 1990-10-12 Oreal PROCESS FOR THE PREPARATION OF ALGINATE (S) CAPSULES PARTICULARLY SUITABLE FOR COSMETIC USE, APPARATUS FOR ITS IMPLEMENTATION AND COSMETIC COMPOSITION CONTAINING SAID CAPSULES
US5204111A (en) * 1989-04-07 1993-04-20 L'oreal Process for the preparation of alginate capsules, apparatus for producing said capsules and cosmetic compositions containing said capsules
EP0391803A1 (en) * 1989-04-07 1990-10-10 L'oreal Process for preparing alginate capsules particularly useful for cosmetics, apparatus for performing said process and cosmetic composition containing said capsules
US6071538A (en) 1992-06-15 2000-06-06 Emisphere Technologies, Inc. Oral delivery composition comprising supramolecular complex
US5578323A (en) 1992-06-15 1996-11-26 Emisphere Technologies, Inc. Proteinoid carriers and methods for preparation and use thereof
US5601846A (en) 1992-06-15 1997-02-11 Emisphere Technologies, Inc. Proteinoid microspheres and methods for preparation and use thereof
US6221367B1 (en) 1992-06-15 2001-04-24 Emisphere Technologies, Inc. Active agent transport systems
US5840340A (en) 1992-06-15 1998-11-24 Emisphere Technologies, Inc. Proteinoid carriers and methods for preparation and use thereof
US6413550B1 (en) 1992-06-15 2002-07-02 Emisphere Technologies, Inc. Proteinoid carriers and methods for preparation and use thereof
US6245359B1 (en) 1992-06-15 2001-06-12 Emisphere Technologies, Inc. Active agent transport systems
US6348207B1 (en) 1992-06-15 2002-02-19 Emisiphere Technologies, Inc. Orally deliverable supramolecular complex
US5788991A (en) * 1993-04-01 1998-08-04 Novartis Corporation Coated microparticle agglomerates
US5643957A (en) 1993-04-22 1997-07-01 Emisphere Technologies, Inc. Compounds and compositions for delivering active agents
US5709861A (en) 1993-04-22 1998-01-20 Emisphere Technologies, Inc. Compositions for the delivery of antigens
US6100298A (en) 1993-04-22 2000-08-08 Emisphere Technologies, Inc. Compounds and compositions for delivering active agents
US5955503A (en) 1993-04-22 1999-09-21 Emisphere Technologies, Inc. Compounds and compositions for delivering active agents
US5792451A (en) 1994-03-02 1998-08-11 Emisphere Technologies, Inc. Oral drug delivery compositions and methods
US5629020A (en) 1994-04-22 1997-05-13 Emisphere Technologies, Inc. Modified amino acids for drug delivery
US6180140B1 (en) 1994-04-22 2001-01-30 Emisphere Technologies, Inc. Modified amino acids for drug delivery
US5935601A (en) * 1994-04-22 1999-08-10 Emisphere Technologies, Inc. Modified amino acids for drug delivery
US5541155A (en) 1994-04-22 1996-07-30 Emisphere Technologies, Inc. Acids and acid salts and their use in delivery systems
US5693338A (en) 1994-09-29 1997-12-02 Emisphere Technologies, Inc. Diketopiperazine-based delivery systems
US5976569A (en) 1994-09-29 1999-11-02 Emisphere Technologies, Inc. Diketopiperazine-based delivery systems
US6331318B1 (en) 1994-09-30 2001-12-18 Emisphere Technologies Inc. Carbon-substituted diketopiperazine delivery systems
US6126936A (en) * 1995-03-10 2000-10-03 Biohybrid Technologies Llc Microcapsules and composite microreactors for immunoisolation of cells
US6346242B1 (en) 1995-03-31 2002-02-12 Emishpere Technologies, Inc. Compounds and compositions for delivering active agents
US6071510A (en) 1995-03-31 2000-06-06 Emisphere Technologies, Inc. Modified amino acids and compositions comprising the same for delivering active agents
US5866536A (en) 1995-03-31 1999-02-02 Emisphere Technologies, Inc. Compounds and compositions for delivering active agents
US6428780B2 (en) 1995-03-31 2002-08-06 Emisphere Technologies, Inc. Compounds and compositions for delivering active agents
US5989539A (en) 1995-03-31 1999-11-23 Emisphere Technologies, Inc. Compounds and compositions for delivering active agents
US6001347A (en) 1995-03-31 1999-12-14 Emisphere Technologies, Inc. Compounds and compositions for delivering active agents
US5650386A (en) 1995-03-31 1997-07-22 Emisphere Technologies, Inc. Compositions for oral delivery of active agents
US5965121A (en) 1995-03-31 1999-10-12 Emisphere Technologies, Inc. Compounds and compositions for delivering active agents
US6090958A (en) 1995-03-31 2000-07-18 Emisphere Technologies, Inc. Compounds and compositions for delivering active agents
US5820881A (en) 1995-04-28 1998-10-13 Emisphere Technologies, Inc. Microspheres of diamide-dicarboxylic acids
US5824345A (en) 1995-06-07 1998-10-20 Emisphere Technologies, Inc. Fragrances and flavorants
US5750147A (en) 1995-06-07 1998-05-12 Emisphere Technologies, Inc. Method of solubilizing and encapsulating itraconazole
US6100285A (en) 1995-06-07 2000-08-08 Emisphere Technologies, Inc. Method of solubilizing itraconazole
US6051258A (en) 1995-06-07 2000-04-18 Emisphere Technologies, Inc. Proteinoid emulsions and methods for preparation and use thereof
US6461545B1 (en) 1995-06-07 2002-10-08 Emisphere Technologies, Inc. Method of solubilizing and encapsulating itraconazole
US6084112A (en) 1995-09-11 2000-07-04 Emisphere Technologies, Inc. Method for preparing ω-aminoalkanoic acid derivatives from cycloalkanones
US6375983B1 (en) 1996-06-14 2002-04-23 Emisphere Technologies, Inc. Microencapsulated fragrances and method for preparation
US6313088B1 (en) 1997-02-07 2001-11-06 Emisphere Technologies, Inc. 8-[(2-hydroxy-4-methoxy benzoyl) amino]-octanoic acid compositions for delivering active agents
US8686154B2 (en) 1997-02-07 2014-04-01 Emisphere Technologies, Inc. Compounds and compositions for delivering active agents
US6242495B1 (en) 1997-02-07 2001-06-05 Emisphere Technologies, Inc. Compounds and compositions for delivering active agents
US5990166A (en) 1997-02-07 1999-11-23 Emisphere Technologies, Inc. Compounds and compositions for delivering active agents
US6060513A (en) 1997-02-07 2000-05-09 Emisphere Technologies, Inc. Compounds and compositions for delivering active agents
US5939381A (en) 1997-02-07 1999-08-17 Emisphere Technologies, Inc. Compounds and compositions for delivering active agents
US5876710A (en) 1997-02-07 1999-03-02 Emisphere Technologies Inc. Compounds and compositions for delivering active agents
US5879681A (en) 1997-02-07 1999-03-09 Emisphere Technolgies Inc. Compounds and compositions for delivering active agents
US5804688A (en) 1997-02-07 1998-09-08 Emisphere Technologies, Inc. Compounds and compositions for delivering active agents
US5863944A (en) 1997-04-30 1999-01-26 Emisphere Technologies, Inc. Compounds and compositions for delivering active agents
US5962710A (en) 1997-05-09 1999-10-05 Emisphere Technologies, Inc. Method of preparing salicyloylamino acids
US6287558B1 (en) 1997-08-01 2001-09-11 Biohybrio Technologies Llc Devices containing cells or tissue and an agent that inhibits damage by a host cell molecule
EP0970623A2 (en) * 1998-07-08 2000-01-12 K.D. Pharma Bexbach GmbH Micro-encapsulated unsaturated fatty acids or derivatives with two polymer layers
EP0970623B1 (en) * 1998-07-08 2005-09-28 K.D. Pharma Bexbach GmbH Micro-encapsulated unsaturated fatty acids or derivatives with two polymer layers
WO2001030146A1 (en) * 1999-10-22 2001-05-03 3M Innovative Properties Company Encapsulated active material immobilized in hydrogel microbeads
US6375968B1 (en) 1999-10-22 2002-04-23 3M Innovative Properties Company Encapsulated active material immobilized in hydrogel microbeads
AU779200B2 (en) * 1999-10-22 2005-01-13 3M Innovative Properties Company Encapsulated active material immobilized in hydrogel microbeads
WO2001064329A1 (en) * 2000-02-29 2001-09-07 Rainer Pommersheim Microcapsule, in particular, for immobilizing organic or inorganic solids, liquids and/or gases
WO2005013941A1 (en) * 2003-08-06 2005-02-17 Fondazione Carlo E Dirce Callerio Onlus Polysaccharide double-layer microcapsules as carriers for biologically active substance oral administration
US10143212B2 (en) 2005-04-26 2018-12-04 Massey University Lipid encapsulation
EP2234711A4 (en) * 2008-01-25 2014-10-08 Reynolds Tobacco Co R Process for manufacturing breakable capsules useful in tobacco products
EP2234711A1 (en) * 2008-01-25 2010-10-06 RJ Reynolds Tobacco Company Process for manufacturing breakable capsules useful in tobacco products
EP3299084A1 (en) * 2008-01-25 2018-03-28 R. J. Reynolds Tobacco Company Process for manufacturing breakable capsules useful in tobacco products
WO2009094859A1 (en) 2008-01-25 2009-08-06 Rj Reynolds Tobacco Company Process for manufacturing breakable capsules useful in tobacco products
EP2364205A2 (en) * 2008-10-17 2011-09-14 Appleton Papers Inc. A fragrance-delivery composition comprising boron and persulfate ion-crosslinked polyvinyl alcohol microcapsules and method of use thereof
EP2364205A4 (en) * 2008-10-17 2014-09-03 Appvion Inc A fragrance-delivery composition comprising boron and persulfate ion-crosslinked polyvinyl alcohol microcapsules and method of use thereof
WO2010044834A2 (en) 2008-10-17 2010-04-22 Appleton Papers Inc. A fragrance-delivery composition comprising boron and persulfate ion-crosslinked polyvinyl alcohol microcapsules and method of use thereof
EP2906050B1 (en) 2012-10-09 2018-04-25 Societe D Exploitation De Produits Pour Les Industries Chimiques Seppic Dietary compositions comprising capsules obtained by coacervation without the use of toxic cross-linking agents
CN108283627A (en) * 2018-04-11 2018-07-17 广西壮族自治区农业科学院农产品加工研究所 A method of preparing starch capsule by major ingredient of hair sweet potato starch

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