CN102964127A - Preparation method of nanometer ceramic powder dispersion liquid and nanometer ceramic powder dispersion liquid - Google Patents
Preparation method of nanometer ceramic powder dispersion liquid and nanometer ceramic powder dispersion liquid Download PDFInfo
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- CN102964127A CN102964127A CN2012104348838A CN201210434883A CN102964127A CN 102964127 A CN102964127 A CN 102964127A CN 2012104348838 A CN2012104348838 A CN 2012104348838A CN 201210434883 A CN201210434883 A CN 201210434883A CN 102964127 A CN102964127 A CN 102964127A
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- ceramic powder
- dispersion liquid
- powder dispersion
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- deionized water
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Abstract
The invention provides a preparation method of nanometer ceramic powder dispersion liquid, comprising the steps of: firstly, dissolving Al2O3 in deionized water, and then instilling a dispersant to prepare a mixed liquid; instilling ammonia water to the mixed liquid to ensure that the pH value of the mixed liquid is 8-9; and carrying out ultrasonic treatment. The nanometer ceramic powder dispersion liquid prepared by using the preparation method comprises the deionized water, Al2O3 and the dispersant, wherein Al2O3 is instilled into the deionized water and then the dispersant is instilled to prepare the mixed liquid; and in the mixed liquid, 5-15g of Al2O3 is dissolved in each 100ml of deionized water and the amount of the instilled dispersant is 1.2-2.4ml. According to the preparation method, the dispersing stability is good, the nanometer ceramic powder dispersion liquid is even and stable, the properties are excellent and relatively good use reliability is provided.
Description
Technical field
The present invention relates to field of printing and dyeing, be specifically related to a kind of preparation method and nano-ceramic powder dispersion liquid of nano-ceramic powder dispersion liquid.
Background technology
The a lot of existence and stabilities of existing nano-ceramic powder dispersion liquid are poor, good poor, the problem that work reliability is poor of properties, can not reach the requirement in some special situation of relaxing.
Summary of the invention
Technical problem to be solved by this invention is to provide a kind of preparation method and nano-ceramic powder dispersion liquid of nano-ceramic powder dispersion liquid, and dispersion stabilization is good, and the nano-ceramic powder dispersion liquid is uniform and stable, properties is good, have preferably work reliability.
For solving above-mentioned existing technical problem, the present invention adopts following scheme: the preparation method of nano-ceramic powder dispersion liquid, and first with Al
2O
3Be dissolved in the deionized water, then splash into dispersion agent and make mixed solution, and then to splash into the pH value that ammoniacal liquor makes mixed solution in the mixed solution be 8 ~ 9, and then carry out ultrasonication.
Adopt the nano-ceramic powder dispersion liquid of above-mentioned preparation method's preparation, comprise deionized water, Al
2O
3And dispersion agent, with Al
2O
3Be dissolved in the deionized water, then splash into dispersion agent and make mixed solution, dissolve in Al in every 100ml deionized water in the described mixed solution
2O
3Amount be 5-15g, the amount that splashes into dispersion agent is 1.2 ~ 2.4ml.
As preferably, dissolve in Al in every 100ml deionized water in the described mixed solution
2O
3Amount be 10g, the amount that splashes into dispersion agent is 2ml, the pH value of described mixed solution is 8.5.
Beneficial effect:
The present invention adopts preparation method and the nano-ceramic powder dispersion liquid of a kind of nano-ceramic powder dispersion liquid that technique scheme provides, and dispersion stabilization is good, and the nano-ceramic powder dispersion liquid is uniform and stable, properties is good, have preferably work reliability.
Embodiment
Embodiment one:
The preparation method of nano-ceramic powder dispersion liquid is first with Al
2O
3Be dissolved in the deionized water, then splash into dispersion agent and make mixed solution, and then to splash into the pH value that ammoniacal liquor makes mixed solution in the mixed solution be 8 ~ 9, and then carry out ultrasonication.
The phenomenons such as sedimentation do not occur in the particle in the nano-ceramic powder dispersion liquid that the preparation method of the described nano-ceramic powder dispersion liquid of employing present embodiment makes, dispersion stabilization is good especially, and the nano-ceramic powder dispersion liquid that makes is uniform and stable, properties is good, have preferably work reliability.
Embodiment two:
Employing comprises deionized water, Al such as the nano-ceramic powder dispersion liquid of preparation method's preparation of nano-ceramic powder dispersion liquid as described in the embodiment one
2O
3And dispersion agent, with Al
2O
3Be dissolved in the deionized water, then splash into dispersion agent and make mixed solution, dissolve in Al in every 100ml deionized water in the described mixed solution
2O
3Amount be 5-15g, the amount that splashes into dispersion agent is 1.2 ~ 2.4ml.Dissolve in Al in every 100ml deionized water in the described mixed solution
2O
3Amount be 10g, the amount that splashes into dispersion agent is 2ml, the pH value of described mixed solution is 8.5.
In the present embodiment, the grain diameter in the nano-ceramic powder dispersion liquid minimum (median size can reach 120nm following), specific surface area are large, and chemical property is good, can make composition densification, the homogenizing of material.
Embodiment three:
Be with the difference of embodiment two: dissolve in Al in every 100ml deionized water in the described mixed solution
2O
3Amount be 5g, the amount that splashes into dispersion agent is 1.2ml, the pH value of described mixed solution is 8.
Embodiment four:
Be with the difference of embodiment two: dissolve in Al in every 100ml deionized water in the described mixed solution
2O
3Amount be 15g, the amount that splashes into dispersion agent is 2.4ml, the pH value of described mixed solution is 9.
Claims (3)
1. the preparation method of nano-ceramic powder dispersion liquid is characterized in that: first with Al
2O
3Be dissolved in the deionized water, then splash into dispersion agent and make mixed solution, and then to splash into the pH value that ammoniacal liquor makes mixed solution in the mixed solution be 8 ~ 9, and then carry out ultrasonication.
2. adopt the nano-ceramic powder dispersion liquid of preparation method's preparation claimed in claim 1, it is characterized in that: comprise deionized water, Al
2O
3And dispersion agent, with Al
2O
3Be dissolved in the deionized water, then splash into dispersion agent and make mixed solution, dissolve in Al in every 100ml deionized water in the described mixed solution
2O
3Amount be 5-15g, the amount that splashes into dispersion agent is 1.2 ~ 2.4ml.
3. nano-ceramic powder dispersion liquid according to claim 2 is characterized in that: dissolve in Al in every 100ml deionized water in the described mixed solution
2O
3Amount be 10g, the amount that splashes into dispersion agent is 2ml, the pH value of described mixed solution is 8.5.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012104348838A CN102964127A (en) | 2012-11-02 | 2012-11-02 | Preparation method of nanometer ceramic powder dispersion liquid and nanometer ceramic powder dispersion liquid |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012104348838A CN102964127A (en) | 2012-11-02 | 2012-11-02 | Preparation method of nanometer ceramic powder dispersion liquid and nanometer ceramic powder dispersion liquid |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN102964127A true CN102964127A (en) | 2013-03-13 |
Family
ID=47794598
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2012104348838A Pending CN102964127A (en) | 2012-11-02 | 2012-11-02 | Preparation method of nanometer ceramic powder dispersion liquid and nanometer ceramic powder dispersion liquid |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103044028A (en) * | 2013-01-24 | 2013-04-17 | 兰州理工大学 | Water-based ZrB2 paste material and preparation method of water-based ZrB2 paste material |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5972820A (en) * | 1997-01-03 | 1999-10-26 | Asec Manufacturing, A General Partnership | Methods of making stabilized crystalline alumina compositions, and alumina compositions and catalyst supports made therefrom |
| CN1513924A (en) * | 2003-05-30 | 2004-07-21 | 中国科学院金属研究所 | Nano-aluminium oxide paste composition and its preparation method |
| CN1887712A (en) * | 2006-07-18 | 2007-01-03 | 中国铝业股份有限公司 | Prepn process of stable alpha-alumina suspension liquid |
| CN101164963A (en) * | 2007-09-26 | 2008-04-23 | 山东轻工业学院 | Micro-nano composite ceramic die material and preparation method thereof |
-
2012
- 2012-11-02 CN CN2012104348838A patent/CN102964127A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5972820A (en) * | 1997-01-03 | 1999-10-26 | Asec Manufacturing, A General Partnership | Methods of making stabilized crystalline alumina compositions, and alumina compositions and catalyst supports made therefrom |
| CN1513924A (en) * | 2003-05-30 | 2004-07-21 | 中国科学院金属研究所 | Nano-aluminium oxide paste composition and its preparation method |
| CN1887712A (en) * | 2006-07-18 | 2007-01-03 | 中国铝业股份有限公司 | Prepn process of stable alpha-alumina suspension liquid |
| CN101164963A (en) * | 2007-09-26 | 2008-04-23 | 山东轻工业学院 | Micro-nano composite ceramic die material and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103044028A (en) * | 2013-01-24 | 2013-04-17 | 兰州理工大学 | Water-based ZrB2 paste material and preparation method of water-based ZrB2 paste material |
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Application publication date: 20130313 |