Search Results (305)

The gradual growth of oxides inside thermal barrier coatings is a key factor leading to the degradation of thermal barrier coating performance until its failure, and accurate monitoring of the growth stress during this process is crucial to ensure the long-term stable operation of engines. In this study, terahertz time-domain spectroscopy was introduced as a new method to characterize the growth stress in thermal barrier coatings. By combining metallographic analysis and scanning electron microscope (SEM) observation techniques, the real microstructure of the oxide layer was obtained, and an accurate simulation model of the oxide growth was constructed on this basis. The elastic solutions of the thermally grown oxide layer of thermal insulation coatings were obtained by using the controlling equations in the rate-independent theoretical model, and the influence of the thickness of the thermally grown oxide (TGO) layer on the stress distribution was explored. Based on experimental data, multidimensional 3D numerical models of thermal barrier coatings with different TGO thicknesses were constructed, and the terahertz time-domain responses of oxide coatings with different thicknesses were simulated using the time-domain finite difference method to simulate the actual inspection scenarios. During the simulation process, white noise with signal-to-noise ratios of 10 dB to 20 dB was embedded to approximate the actual detection environment. After adding the noise, wavelet transform (WT) was used to reduce the noise in the data. The results showed that the wavelet transform had excellent noise reduction performance. For the problems due to the large data volume and small sample data after noise reduction, local linear embedding (LLE) and kernel-based extreme learning machine (KELM) were used, respectively, and the kernel function was optimized using the gray wolf optimization (GWO) algorithm to improve the model’s immunity to interference. Experimental validation showed that the proposed LLE-GWO-KELM hybrid model performed well in predicting the TGO growth stress of thermal insulation coatings. In this study, a novel, efficient, nondestructive, online, and high-precision measurement method for the growth in TGO stress of thermal barrier coatings was developed, which provides reliable technical support for evaluating the service life of thermal barrier coatings. Full article

Directed Energy Deposition Laser Beam (DED-LB) is a promising additive manufacturing technique that uses a laser source and a powder stream to build or repair metal components. Repair applications offer significant economic and environmental benefits but are more challenging to develop, especially for components that are difficult to process due to their intricate geometries and materials. Process conditions can change precipitously, and it is essential to implement monitoring systems that ensure high process stability and, consequently, superior end-product quality. In the present work, a mid-wave infrared coaxial camera was used to monitor the melt pool geometry. To simulate the challenging repair process conditions of the DED-LB process, experimental tests were carried out on substrates with different thicknesses. The stability of the deposition process on nickel-based superalloys was analyzed by means of MATLAB algorithms. Thus, the effect of open-loop and closed-loop monitoring with back control on laser power on the process conditions was assessed and quantified. Metallographic analysis of the produced samples was carried out to validate the analyses performed by the monitoring system. The occurrence of production defects (lack of fusion and porosity) related to parameters not directly controllable by monitoring systems, such as penetration depth and dilution, was determined. Full article

This article introduces a novel approach for assessing microstructure, particularly its degradation after extended operation. The authors focus on creep processes in power plant components, highlighting the importance of diagnostics in this field. This article emphasizes the value of combining traditional microstructure observation techniques with image analysis. A non-destructive method of evaluating microstructure parameters (matrix replicas) is presented, and its accuracy is evaluated against the conventional destructive method. The assessment utilizes quantitative data derived from classical stereological principles and image analysis. Parameters like mean chord length, relative surface area, mean cross-sectional area, and mean equivalent diameter are compared for replica and metallographic specimens. The results show that the replica method accurately reproduces the microstructure. In their conclusions, the authors highlight the importance of developing visual methods alongside the application of artificial intelligence while indicating the challenges in achieving this goal. Full article

In Laser Powder Bed Fusion, process material defects such as a lack of fusion, powder inclusions and cavities occur repeatedly by chance. These stochastically distributed defects can significantly reduce the mechanical performance of the components during operation. Possible in situ repair solutions such as multiple remelting of specific layer areas are promising approaches to avoid these defects in the finished component, thus improving the overall properties. In this context, the present study investigates the remelting of artificially introduced defects using the example of M789 tool steel. In the first step, the process parameter settings and mechanical properties were evaluated using a tensile test, and the density of the local repair was examined using X-ray computer tomography and a metallographic analysis. The results demonstrate that the mechanical properties of the tensile test are comparable with those of the reference samples while successfully increasing the component quality. This indicates that defects that arise during the process can be remelted without the loss of mechanical characteristics. Full article

Duralumin-type alloys have been employed for structural and non-structural parts of aircraft since the early 1920s up to now. In the European project “PROtection and Conservation of Heritage AirCRAFT” (PROCRAFT), up to 34 aircraft wrecks from World War II from different nations (United States of America, United Kingdom, France, Germany, Italy) were identified. On most of them, the collection of numerous fragments was possible, thus constituting a large sampling group. A metallographic analysis was carried out, and elemental composition, microstructure and hardness were measured. This article focuses firstly on the elemental composition of this group of historical Al alloys. From these data, some fine characteristics specific to the manufacturing countries will be investigated through principal component analysis. Then, on a restricted group constituted of German alloys, we will discuss how some manufacturing parameters, such as micro-alloying and thermo-mechanical treatments, influence the mechanical properties of the assessed aircraft components. Other influencing parameters, linked to the archaeological nature of the parts, are considered and addressed based on a specific study of an alloy collected on a crashed JU88 aircraft originating from the German company Junkers. Full article

A high-noble Au–Pt–Ge porcelain-fused-to-metal (PFM) dental alloy without the known adverse metallic elements and with the addition of germanium (Ge) was produced as a more cost-effective alternative to other precious alloying metals, with investigations for determining the functionality and clinical use of this alloy. The thermomechanical, biocompatibility, durability, workability and economic characteristics of the produced dental alloy were investigated. These properties were investigated with in vitro biocompatibility testing on human gingival fibroblasts (HGFs); static immersion testing for metal ion release; DSC analysis; hardness, tensile testing, density and coefficient of thermal expansion (CTE) measurements; metallographic and SEM/EDX microstructure investigations; and finally with the production of a test PFM dental bridge. The results of the thermomechanical testing showed alloy properties suitable for dental restorations and clinical use, with somewhat lower mechanical properties, making the alloy not suitable for extensive multiunit fixed restorations. The microstructure investigations showed segregations of Ge in the homogeneous alloy matrix, which reduce the alloy’s mechanical properties. The produced PFM dental bridge showed excellent workability of the alloy in a dental laboratory setting, as well as a high standard of the final dental restoration. The ion release was negligible, well below any harmful quantities, while the cell viability examination showed significantly higher viability ratings on polished alloy samples as compared to as-cast samples. The results showed that a dental substructure in direct contact with oral tissue and fluids should be highly polished. The performed investigations showed that the produced PFM dental alloy is suitable for clinical use in producing high-quality dental restorations with high biocompatibility for patients prone to metal allergies. Full article

The main objective of this research is to conduct an experimental investigation of the bimetallic material formed by 316LSI stainless steel and S275JR structural steel, produced via hybrid wire arc additive manufacturing technology with cool metal transfer welding and machining, and with the objective of being able to reduce the industrial cost of certain requirements for one of the materials. A methodological investigation has been carried out starting with welding beads of 316LSI on S275JR plates, followed by overlapping five beads and conducting final experiments with several vertical layers, with or without intermediate face milling. The results achieved optimal bead conditions for wire speeds of 4 m/min and 5 m/min at a travel speed of 400 mm/min. Overlap experiments show that the best deposition results are obtained with an overlap equal to or greater than 28%. Cooling time does not significantly influence the final geometry of the coatings. Regarding metallographic analysis, the filler material presents an austenitic columnar structure. In the base material, a bainitic structure with inferred grain refinement was detected in the heat-affected zone. An increase in hardness is observed in the heat-affected zone. In the results obtained from the tensile tests of the bimetallic material, an increase in mechanical strength and yield strength is observed in the tested specimens. Full article

This paper explores the evolving significance of metal injection molding (MIM) technology, particularly as a promising alternative for the precise and cost-effective manufacturing of small-scale, high-volume products in the automotive industry. Despite its growing adoption, the quality control processes for intermediate “green” parts and the final metal products are not yet well established, posing significant challenges in ensuring product reliability and consistency. Furthermore, the research thoroughly examines the recycling of MIM feedstock and its impact, especially on the change in carbon content. Scanning Electron Microscopy (SEM) images were taken of the samples, the chemical composition was analyzed using Energy-Dispersive X-ray Spectroscopy (EDX), and the pearlitic regions of samples from different generations were compared using image analysis software on microscopic cross-sections. Full article

Accurately characterizing the internal porosity rate of thermal barrier coatings (TBCs) was essential for prolonging their service life. This work concentrated on atmospheric plasma spray (APS)-prepared TBCs and proposed the utilization of terahertz non-destructive detection technology to evaluate their internal porosity rate. The internal porosity rates were ascertained through a metallographic analysis and scanning electron microscopy (SEM), followed by the reconstruction of the TBC model using a four-parameter method. Terahertz time-domain simulation data corresponding to various porosity rates were generated employing the time-domain finite difference method. In simulating actual test signals, white noise with a signal-to-noise ratio of 10 dB was introduced, and various wavelet transforms were utilized for denoising purposes. The effectiveness of different signal processing techniques in mitigating noise was compared to extract key features associated with porosity. To address dimensionality challenges and further enhance model performance, kernel principal component analysis (kPCA) was employed for data processing. To tackle issues related to limited sample sizes, this work proposed to use the Siamese neural network (SNN) and generative adversarial network (GAN) algorithms to solve this challenge in order to improve the generalization ability and detection accuracy of the model. The efficacy of the constructed model was assessed using multiple evaluation metrics; the results indicate that the novel hybrid WT-kPCA-GAN model achieves a prediction accuracy exceeding 0.9 while demonstrating lower error rates and superior predictive performance overall. Ultimately, this work presented an innovative, convenient, non-destructive online approach that was safe and highly precise for measuring the porosity rate of TBCs, particularly in scenarios involving small sample sizes facilitating assessments regarding their service life. Full article

Aiming to address the wear and replacement inconvenience of concrete mixer liners, this study utilizes a laser cladding system to clad Fe60 alloy powder on the liner. It investigates the influence of different process parameters on the forming quality of the Fe60 alloy powder cladding layer. The optimal process parameters were obtained by weighted comprehensive evaluation, and single-layer multi-pass cladding experiments were carried out under the optimal process parameters to investigate the effects of a 30%, 40%, and 50% lap rate on the surface flatness and forming quality of the cladding layer. Using a metallographic microscope, a scanning electron microscope analysis of the macro morphology and microstructure of the cladding layer was conducted, a DPT-5 penetration flaw detector was used to observe the cracks on the surface of the multi-channel cladding, a microhardness tester and friction and wear experimental machine were used for the hardness of the cladding layer, and an abrasive wear resistance test was conducted. The results show that under the process parameters of a laser power of 900 W, powder feeding speed of 7 g/min, scanning speed of 600 mm/min, and 50% lap rate, the average microhardness of the fused cladding layer reaches 742 HV, which is 1.8 times higher than that of the liner plate, and the coefficient of friction is 0.57, which improves the liner plate’s wear resistance performance and service life. Full article

The introduced work deals with the microscopic analysis of metallographically prepared selected metal materials structures, using a scanning electron microscope (SEM). Prepared samples of seamless steel pipes were subjected to a thorough microscopic examination from the outer surface to the inner regions in order to interpret the specific structure, including the change in the inner surfaces due to wear. The experiment demonstrated that the microstructure and character of the surfaces play a key role in the behavior of metallic materials in real conditions of hot water heating. Four pipe samples were monitored according to their use. The unused steel pipe (designated as sample No. 1) exhibited a rough outer surface with identified inclusions, while the used pipe (designated as sample No. 2) showed marks of intergranular corrosion and significant wear after long-term use. The older pipe (designated as sample No. 3) showed a decarburized area and inclusions containing sulfides and aluminum. The steel pipe with corrosion layers (designated as sample No. 4) exhibited a continuous corrosion layer with cavitation and cracks. The results of this study offer a comprehensive view of the influence of the nature of microstructure and wear on water flow in metal pipes, with an emphasis on the identification of possible risks associated with geometry change, corrosion, and wear. The findings form the basis for predicting degradation and appropriate maintenance in order to ensure their long and reliable service life under real conditions of use. They offer the possibility of continuing and expanding research and analysis of the use of metallic materials in comparison with polymers and composites. Full article

Copper-based composites with enhanced strength and conductivity are critically important for improving efficiency and reducing energy consumption in the energy and power industries. However, scalable production of copper-based composites that simultaneously enhance both conductivity and strength through conventional methods remains a significant challenge. This work explores the synthesis of high-quality graphene/copper (Gr/Cu) composite powders using in situ chemical vapor deposition (CVD). These powders were further processed through powder metallurgy and annealing techniques to produce wires with both high conductivity and increased mechanical strength. The morphology, structure and properties of Gr/Cu composite powders with different morphologies and graphene content were systematically analyzed by means of advanced characterization technology and metallographic structure analysis. The integration of high-quality graphene not only facilitated rapid electron transfer pathways but also enhanced mechanical properties through mechanisms such as grain refinement and load transfer. The produced annealed Gr/Cu composite wires exhibited electrical conductivities exceeding 100% International Annealed Copper Standard (IACS) and tensile strengths above 238 MPa. These findings are vital for the development of a new generation of high-conductivity electrical copper materials and products, contributing to the restructuring of energy resources and advancing the electrical copper industry. Full article

In order to improve the tribological properties of the 7075-T6 aluminum alloy used on the rotor surface, a combined method of cryogenic treatment and laser surface texture treatment was applied. Various tests, including metallographic microscopy, scanning electron microscopy, elemental analysis, microhardness measurements, were conducted to examine the wear morphology and modification mechanism of the treated 7075-T6 aluminum alloy surface. A numerical simulation model of surface texture was established using computational fluid dynamics to analyze the lubrication characteristics of V-shaped texture. The research finding that the 7075-T6 aluminum alloy experienced grain refinement during the cryogenic treatment process, enhancing the wear resistance of the V-shaped textures. This improvement delayed the progression of fatigue wear, abrasive wear, and oxidative wear, thereby reducing friction losses. The designed V-shaped texture contributes to reducing contact area, facilitating the capture and retention of abrasives, and enhancing oil film load-bearing capacity, thereby improving tribological performance. The synergistic effect of cryogenic treatment reduced the friction coefficient by 24.8% and the wear loss by 66.4%. Thus, the combination of surface texture and cryogenic treatment significantly improved the tribological properties of the 7075-T6 aluminum alloy. Full article

This study utilized a bobbin tool to friction stir weld aluminum 6082 workpieces under two sets of process parameters: a tool rotation speed of 280 rev/min with a weld velocity of 280 mm/min (280/280) and a tool rotation speed of 450 rev/min with a weld velocity of 450 mm/min (450/450). The weld microstructures were characterized through optical microscopy utilizing polarized light and through transmission electron microscopy (TEM) and scanning electron microscopy (SEM) coupled with chemical analysis by energy dispersive spectroscopy and electron back scatter diffraction. The microstructural studies were supplemented by hardness measurements (Vickers) performed on the same sections as the metallographic examinations. The produced weldments were free from cracks and any discontinuities. Fine, equiaxed grains that were several microns in size characterized the stir zones (SZs), and the advancing (AS) and retreating (RS) sides revealed distinct microstructural features. On the AS, the transition from the thermo-mechanically affected zone to the SZ was well defined and sharp, but on the RS, the transition appeared as a continuous, gradual change in microstructure. The lower weld energy (280/280) produced lower hardness in the stir zone than the higher energy weld (450/450), ~95 HV1 versus ~115 HV1; however, the 280/280 welds showed higher tensile strengths than the 450/450 welds, ~238 MPa as opposed to ~172 MPa. These behaviors in mechanical performance correlated with the temperature histories produced by each set of weld parameters in relation to the precipitation behavior of the alloy. The fracture characteristics of the weldments were notably different with the 450/450 sample fracturing in a quasi-brittle manner with slight plastic deformation and the 280/280 sample fracturing ductilely. A numerical simulation supported the investigation by elucidating the temperature and material flow behavior during the joining process. Full article

Improving the competitiveness of steel companies is linked to sustainable, quality-compliant steel production. Therefore, new steel production technologies contributing to increased cleanliness of steel are continuously being developed and optimized. One way to achieve a high steel quality is to use electro slag remelting (ESR) technology. In this paper, the principle of ESR technology and the importance of fused slags for optimizing the process are outlined. The aim of this work was to analyze the main thermophysical properties of steel and fused slags used in the ESR process. Determination of the properties of steel and slags was performed using the FactSage calculation software, which involved the calculation of the liquid and solid temperature of steel and slags, the calculation and construction of quaternary diagrams, and the calculation of viscosity. The resulting quaternary diagrams revealed the substantial influence of chemical composition on melting temperatures of slags. In order to validate the acquired results, a CrNiMoV-type steel was subjected to investigation of its metallographic cleanliness and evaluation of its mechanical properties; the ESR process was shown to significantly improve the cleanliness of the steel and improve the mechanical properties of the steel compared to its cleanliness and quality when produced via vacuum degassing (VD) technology. During the ESR process, the average size of non-metallic inclusions was reduced from 20 μm to 10 μm, and the maximum size of non-metallic inclusions was reduced from 50 μm to 28 μm. The mechanical properties of the steel produced using ESR technology were impacted as follows: the ductility increased by 10%, contraction increased by 18%, notched toughness at 20 °C increased by 46%, and at −40 °C (respectively −50 °C) it increased by 30%. Full article