Search Results (6,563)

The fabrication of stable, tailored domain patterns in ferroelectric crystals has wide applications in optical and electronic industries. All-optical ferroelectric poling by pulse laser irradiation has been developed recently. In this work, we studied the creation of the domain structures in MgO-doped lithium tantalate by focused irradiation with a femtosecond near-infrared laser. Cherenkov-type second harmonic generation microscopy was used for domain imaging of the bulk. We have revealed the creation of enveloped domains around the induced microtracks under the action of the depolarization field. The domain growth is due to a pyroelectric field caused by a nonuniform temperature change. The domains in the bulk were revealed to have a three-ray star-shaped cross-section. It was shown that an increase in the field excess above the threshold leads to consequential changes in domain shape from a three-ray star to a triangular and a circular shape. The appearance of comb-like domains as a result of linear scanning was demonstrated. All effects were considered in terms of a kinetic approach, taking into account the domain wall motion by step generation and kink motion driven by excess of the local field over the threshold. The obtained knowledge is useful for the all-optical methods of domain engineering in ferroelectrics. Full article

New developments in nickel-based superalloys and production methods, such as the use of additive manufacturing (AM), can result in innovative designs for turbines. It is crucial to understand how the material behaves during the AM process to advance the industrial use of these techniques. An analytical model based on reaction–diffusion formalism is developed to better explain the solidification behavior of the material during laser metal deposition (LMD). The well-known Scheil–Gulliver theory has some drawbacks, such as the assumption of equilibrium at the solid–liquid interface, which is addressed by this method. The solidified fractions under the Scheil model and the pure equilibrium model are calculated using CALPHAD simulations. A differential scanning calorimeter is used to measure the heat flow during the solid–liquid phase transformation, the result of which is further converted to solidified fractions. The analytical model is compared with all the other models for validation. Full article

A complementary characterisation of the Al-alloy EN AW-5454 was carried out, intended for obtaining the laser hybrid welding parameters of subassemblies in the automotive industry. The investigation included a microstructural examination and the determination of the alloy’s properties using several analytical methods (HV5 hardness measurement, tensile test, Charpy impact toughness, fracture mechanics analysis). Samples were prepared in the longitudinal and transverse directions of a cold-rolled sheet of EN AW-5454 with thicknesses of 3.5 mm and 4 mm. The measured hardness on the thinner sheet was 5% higher than on the thicker sheet. The tensile and yield strength were nominal, while the elongations were smaller by 2.2–3.2% for the longitudinal samples and by 2.7–13.7% for the transverse samples. The smaller deviations from the nominal values are for the thinner sheet metal. A precise topographical analysis showed the brittle fractures of the samples. The Charpy impact toughness results on the thicker plate showed a 20% greater work needed to break it in the longitudinal direction than in the transverse direction. With the thinner sheet metal, 40% greater work was needed. SEM (scanning electron microscope) analysis has shown that the intermetallic Al₆(Mn,Fe) particles in the longitudinal samples were mostly intact, with evidence of tough areas on the upper part of the fracture, indicating a better toughness than the specimens in the transverse direction. More crushed intermetallic particles were observed at the fractures of the transverse samples, and their distribution appeared to be more oriented in the direction of rolling. Fracture mechanics SENB (single edge notch bending) tests and their analysis showed that the resistance of the material to crack propagation in the longitudinal sample was about 50% greater than that in the transverse sample. SEM analysis of the fractures showed that the state of the intermetallic particles in the fracture mechanics testing and the fracture mechanism differed from the one in the Charpy fractures. Full article

In order to enhance the application of thermoregulated materials, magnetic phase change microcapsules were prepared using a self-assembly method. Paraffin wax was chosen for its fine thermoregulation properties as the core material, while Fe₃O₄ nanoparticles doped in calcium carbonate served as the hybrid shell material. The microcapsules were then blended with sodium alginate and processed into seaweed fibers through wet spinning. The microstructure, thermal, and magnetic properties of the microcapsules were analyzed using scanning electron microscopy, energy dispersive X-ray spectroscopy, a laser particle size analyzer, an X-ray diffractometer, a differential scanning calorimeter, a thermogravimetric analyzer, and a vibrating sample magnetometer. The thermoregulation of the fibers was evaluated using a thermal infrared imager. The results indicated that the microcapsules had a uniform size distribution and good thermal properties. When the mass fraction of Fe₃O₄ nanoparticles was 8%, the microcapsules exhibited a saturation magnetization of 2.44 emu/g and an enthalpy value of 94.25 J/g, indicating effective phase change and magnetic properties. Furthermore, the thermoregulated seaweed fibers showed a high enthalpy value of 19.8 J/g with fine shape, offering potential for developing multifunctional fiber products. Full article

In order to improve the tribological properties of the 7075-T6 aluminum alloy used on the rotor surface, a combined method of cryogenic treatment and laser surface texture treatment was applied. Various tests, including metallographic microscopy, scanning electron microscopy, elemental analysis, microhardness measurements, were conducted to examine the wear morphology and modification mechanism of the treated 7075-T6 aluminum alloy surface. A numerical simulation model of surface texture was established using computational fluid dynamics to analyze the lubrication characteristics of V-shaped texture. The research finding that the 7075-T6 aluminum alloy experienced grain refinement during the cryogenic treatment process, enhancing the wear resistance of the V-shaped textures. This improvement delayed the progression of fatigue wear, abrasive wear, and oxidative wear, thereby reducing friction losses. The designed V-shaped texture contributes to reducing contact area, facilitating the capture and retention of abrasives, and enhancing oil film load-bearing capacity, thereby improving tribological performance. The synergistic effect of cryogenic treatment reduced the friction coefficient by 24.8% and the wear loss by 66.4%. Thus, the combination of surface texture and cryogenic treatment significantly improved the tribological properties of the 7075-T6 aluminum alloy. Full article

Rail infrastructure plays an important role in fulfilling the demand for freight and passenger transportation. Increases in traffic volume, heavier axles and vehicles, higher speeds, and increasing climate extremes all contribute to the constant strain on the infrastructure. Due to their major importance in the transportation of people and freight, they are subject to continuous condition monitoring. This is an essential requirement for the selective planning of maintenance tasks and ultimately for safe and reliable operation. Various measuring systems have been developed for this purpose. These must measure precisely, quickly, and robustly under difficult conditions. Whether installed from mobile or stationary platforms, they have to cope with a wide range of ambient temperatures and lighting conditions, harsh environmental influences, and varying degrees of reflection. Despite these circumstances, railway operators require precise measurement data, high data densities even at high traveling speeds, and a user-friendly presentation of the results. Photogrammetry, laser scanning, and fiber optics are light-based measurement methods that are used in this sector. They are able to record with high precision rail infrastructure such as overhead contact systems, clearance profiles, rail tracks, and much more. This article provides an overview of the established and modern optical sensing methods, as well as the use of artificial intelligence as an evaluation method, and highlights their advantages and disadvantages. Full article

The knowledge of the deposition fate of ambient polycyclic aromatic hydrocarbons (PAHs) on plant leaves is limited. To fill in this knowledge gap, this study strives to observe the intermolecular complex between the polycyclic aromatic hydrocarbons and epicuticular wax of plant leaves using laser scanning microscopy. Epicuticular wax refers to a type of organic mixture that covers the outermost layer of leaves. The leaves of 20 tree species were collected in Beijing in July 2023. The concentrations of 31 PAHs were quantified by gas chromatography–mass spectrometry. Furthermore, the intermolecular complexes of polycyclic aromatic hydrocarbons and epicuticular wax were found with a fluorescence spectrofluorometer and laser scanning microscopy. The levels of total PAHs across 20 tree species ranged from 12.4 ng g⁻¹ to 68.4 ng g⁻¹. Differences in the amounts of total PAHs across tree leaves were observed, which may be ascribed to the differences in leaf surface across tree types. The higher concentration of low-molecular-weight PAHs was found in leaves compared to high-molecular-weight PAHs. The fluorescence spectrofluorometer identified the formation of a new intermolecular complex with fluorescence emission at an excitation wavelength of 340 nm between PAHs and epicuticular wax relative to PAHs. We used laser scanning microscopy with a 405 nm laser for excitation to observe the new intermolecular complex of PAHs and epicuticular wax on the stomata and epicuticular wax of leaves. This study found the intermolecular complex of PAHs on the surface of leaves in situ, which provides important information about the deposition fate of ambient PAHs. Full article

Oily sludge (OS) has long been regarded as a hazardous waste, and improper disposal may lead to serious environmental concerns and human health risks. Despite various methods having been proposed and applied to the treatment of OS, the oil occurrence states and properties in sludge are rarely characterized, which may directly link to the selection and effectiveness of treatment methods. Here, confocal laser scanning microscopy (CLSM), X-ray diffraction (XRD), gas chromatography (GC), and four components (SARA) analysis were utilized to characterize the changes in the oil occurrence states and compositions in OS samples before and after high-speed stirring (HSS) treatment. Our results show a substantial reduction in the oil concentration of OS after HSS treatment (from 32.98% to 1.65%), while SARA analysis reveals a similar oil composition before and after treatment, suggesting the broad applicability of HSS in removing oil and its insignificant selectivity towards various hydrocarbon components. This is further supported by the total petroleum hydrocarbon (TPH) analysis results, which show that the separated oil phase has a hydrocarbon composition similar to that of the original OS sample. The CLSM and fluorescence analysis suggest a homogeneous distribution of oil in the sludge, with relatively light components more concentrated in the pore systems between coarse mineral particles, whereas relatively heavy components tend to coexist with clay minerals. After HSS cleaning, both light and heavy components are removed to varying degrees, but light components are preferentially removed while heavy components tend to be retained in the sludge due to adsorption by clay minerals. This is consistent with TPH analysis, where a significant decrease in n-alkanes with lower carbon numbers (n-C14 to n-C20) was observed in the residual sample. Our findings demonstrate the dynamic response of oil occurrence states and compositions to the OS treatment process and highlight the importance of characterizing these fundamental properties prior to the selection of OS treatment methods. Full article

Radiative transfer models (RTMs) are often used to retrieve biophysical parameters from earth observation data. RTMs with multi-temporal and realistic forest representations enable radiative transfer (RT) modeling for real-world dynamic processes. To achieve more realistic RT modeling for dynamic forest processes, this study presents the 3D-explicit reconstruction of a typical temperate deciduous forest in 2015 and 2022. We demonstrate for the first time the potential use of bitemporal 3D-explicit RT modeling from terrestrial laser scanning on the forward modeling and quantitative interpretation of: (1) remote sensing (RS) observations of leaf area index (LAI), fraction of absorbed photosynthetically active radiation (FAPAR), and canopy light extinction, and (2) the impact of canopy gap dynamics on light availability of explicit locations. Results showed that, compared to the 2015 scene, the hemispherical-directional reflectance factor (HDRF) of the 2022 forest scene relatively decreased by 3.8% and the leaf FAPAR relatively increased by 5.4%. At explicit locations where canopy gaps significantly changed between the 2015 scene and the 2022 scene, only under diffuse light did the branch damage and closing gap significantly impact ground light availability. This study provides the first bitemporal RT comparison based on the 3D RT modeling, which uses one of the most realistic bitemporal forest scenes as the structural input. This bitemporal 3D-explicit forest RT modeling allows spatially explicit modeling over time under fully controlled experimental conditions in one of the most realistic virtual environments, thus delivering a powerful tool for studying canopy light regimes as impacted by dynamics in forest structure and developing RS inversion schemes on forest structural changes. Full article

Tactile maps are widely recognized as useful tools for mobility training and the rehabilitation of visually impaired individuals. However, current tactile maps lack real-time versatility and are limited because of high manufacturing and design costs. In this study, we introduce a device (i.e., ClaySight) that enhances the creation of automatic tactile map generation, as well as a model for wearable devices that use low-cost laser imaging, detection, and ranging (LiDAR,) used to improve the immediate spatial knowledge of visually impaired individuals. Our system uses LiDAR sensors to (1) produce affordable, low-latency tactile maps, (2) function as a day-to-day wayfinding aid, and (3) provide interactivity using a wearable device. The system comprises a dynamic mapping and scanning algorithm and an interactive handheld 3D-printed device that houses the hardware. Our algorithm accommodates user specifications to dynamically interact with objects in the surrounding area and create map models that can be represented with haptic feedback or alternative tactile systems. Using economical components and open-source software, the ClaySight system has significant potential to enhance independence and quality of life for the visually impaired. Full article

Rail surface cracks are widespread damage that can lead to uneven surfaces of railheads and affect traveling safety. Non-destructive testing is needed to inspect rails regularly to ensure the normal operation of railroads. This paper proposes a laser ultrasonic testing method combining variational mode decomposition and diffractive Rayleigh wave time-of-flight to detect tiny cracks on the rail surface quantitatively. The finite element method was combined with experiments to simulate and experimentally investigate cracks of different sizes numerically. In the numerical simulation, the location of the crack was determined by B-scan. Afterward, the interaction between various types of ultrasound and cracks was comparatively analyzed, and the crack size was quantitatively characterized using useful information from the ultrasound signals. The results show that the time-of-flight method can detect arbitrary cracks with low error. Therefore, the experimentally acquired ultrasound signals used the time difference between the diffracted Rayleigh wave and other ultrasound waves to detect the crack information quantitatively. The variational mode decomposition method was used to separate the ultrasonic signals and extract the best surface wave modes to improve the signal-to-noise ratio. The results show that the combination of variational mode decomposition and time-of-flight method can effectively detect the size of cracks. Full article

Background and Objectives: This research investigated the morphometric dimensions of the optic foramen (OF), superior orbital fissure (SOF) and inferior orbital fissure (IOF), using indirect measurement techniques such as laser scanning, making it likely the first study of its kind. This study aimed to identify the morphometric variability of the main orbit communications and to highlight the differences between genders. Materials and Methods: The anthropometric study was conducted on sixty dry skulls (120 orbits) of adults aged between 20 and 70 years. Measurements of orbital communications were made using the RS6 laser scanner. The orbital parameters that were investigated are as follows: length and width of the SOF and IOF, and height and width of the OF. Results: In males, the average height of the OF was 8.27 mm and 8.13 mm in females, while the average width of the OF was 6.34 mm in males and 5.83 mm in females. The SOF average length was 21.09 mm in males and 17.58 mm in females. The widths of the SOF in the three thirds (anterior, middle and posterior) in males were 5.14/4.77/7.11 mm and 2.28/3.48/5.80 mm in females. The average length of the IOF was 33.05 mm in males and 32.30 mm in females. The widths of the IOF in the three thirds (anterior, middle and posterior) were 5.61/3.92/4.70 mm in males and 7.24/4.68/4.08 mm in females. Conclusions: The OF height and width were higher in males compared to females. The SOF length and width were higher in males compared to females. The IOF length was higher in males for the right orbit and higher in females for the left orbit. The IOF width for both orbits was higher in females in the anterior and middle third, and higher for males in the posterior third. Evaluation of dry skulls using laser scanning is reliable and recommended for data accuracy. Laser scanning can become a usable method for all indented and hard-to-reach regions of the cranial skeleton. Full article

Due to energy shortages and the greenhouse effect, the efficient use of energy through phase-change materials (PCMs) is gaining increased attention. In this study, magnetic phase-change microcapsules (Mag-mc) were prepared by suspension polymerization. The shell layer of the microcapsules was formed by copolymerizing methyl methacrylate and triethoxyethylene silane, with the latter enhancing the compatibility of the shell layer with the magnetic additive. Ferric ferrous oxide modified by oleic acid (Fe₃O₄(_m)) was added as the magnetic additive. Differential scanning calorimetry (DSC) testing revealed that the content of phase-change materials in microcapsules without and with ferric ferrous oxide were 79.77% and 96.63%, respectively, demonstrating that the addition of Fe₃O₄(_m) improved the encapsulation efficiency and enhanced the energy storage ability of the microcapsules. Laser particle size analysis showed that the overall average particle sizes for the microcapsules without and with ferric ferrous oxide were 3.48 μm and 2.09 μm, respectively, indicating that the incorporation of magnetic materials reduced the size and distribution of the microcapsules. Thermogravimetric analysis indicated that the thermal stability of the microcapsules was enhanced by the addition of Fe₃O₄(_m). Moreover, the infrared emissivity of the microcapsule-containing film decreased from 0.77 to 0.72 with the addition of Fe₃O₄(_m) to the shell of microcapsules. Full article

In this study, the geomorphological evolution of an inner flank of the Dolomieu at Piton de La Fournaise/La Réunion was investigated with the help of terrestrial laser scanning (TLS) data, terrestrial photogrammetric images, and historical webcam photographs. While TLS data and the terrestrial images were recorded during three field surveys, the study was also able to use historical webcam images that were installed for the monitoring of the volcanic activity inside the crater. Although the webcams were originally intended to be used only for visual monitoring of the area, at certain times they captured image pairs that could be analyzed using structure from motion (SfM) and subsequently processed to create digital terrain models (DTMs). With the help of all the data, the geomorphological evolution of selected areas of the crater was investigated in high temporal and spatial resolution. Surface changes were detected and quantified on scree slopes in the upper area of the crater as well as on scree slopes at the transition from the slope to the crater floor. In addition to their quantification, these changes could be assigned to individual geomorphological processes over time. The webcam photographs were a very important additional source of information here, as they allowed the observation period to be extended further into the past. Besides this, the webcam images made it possible to determine the exact dates at which geomorphological processes were active. Full article

Investment casting is a widely utilized casting technique that offers superior dimensional accuracy and surface quality. In this method, the wax patterns are employed in the layer-by-layer formation of a shell mold. As is customary, the patterns were created through the injection of molten or semi-solid wax into the die. The quality of the final casting is affected by the quality of the wax pattern. Furthermore, the filling of the die with wax can be associated with die-filling challenges, such as the formation of weld lines and misruns. In this study, the injection filling of the fluidity probe die with RG20, S1235, and S1135 pattern waxes was simulated using ProCast software. The thermal properties of the waxes, including thermal conductivity, heat capacity, and density across a wide temperature range, were determined with the assistance of a laser flash analyzer, a differential scanning calorimeter, and a dynamic mechanical analyzer. A favorable comparison of the acquired properties with those reported in the literature was observed. The Carreau model, which corresponds to non-Newtonian flow, was employed, and the parameters in the Carreau viscosity equation were determined as functions of temperature. Utilizing the thermal data associated with the wax patterns and the simulation outcomes, the interfacial heat transfer coefficients between the wax and the die were ascertained, yielding a value of 275–475 W/m²K. A strong correlation was observed between the experimental and simulated filling percentages of the fluidity probe across a wide range of injection temperatures and pressures. The analysis of the simulated temperature, fraction solid, viscosity, and shear rate in the wax pattern revealed that viscosity is a crucial factor influencing the wax fluidity. It was demonstrated that waxes with an initial high viscosity exhibit a low shear rate, which subsequently increases the viscosity, thereby hindering the wax flow. Full article